چکیده :

Poly(N-bromoacrylamide) (PNBA) was prepared and used as a heterogeneous electrophilic catalyst under solvent-free and microwave conditions for the mild and efficient protection of carbonyl compounds as their dithiolane, dithiane and oxathiolane derivatives with 1,2-ethanedithiol, 1,3-propanedithiol and 2-mercaptoethanol, respectively in good to excellent yields. This method is simple, efficient and straightforward for synthesis of 1,3-oxathiolanes, 1,3-dithiolanes and 1,3-dithianes from carbonyl compounds. The catalyst is recoverable and reusable

کلید واژگان :

Poly(N-bromoacrylamide), Heterogeneous catalyst, Protection, Dithioacetal, Solvent free, Microwave



ارزش ریالی : 600000 ریال
دریافت مقاله
با پرداخت الکترونیک